Lab-scale twin-screw micro-compounders as a new rubber-mixing tool: 'a comparison on EPDM/carbon black and EPDM/silica composites'

Official URL: https://dx.doi.org/10.3390/polym13244391

The research and development (R&D) in rubber formulation development require reproducible, repeatable, fast, accurate, and efficient sample preparation. The lab-scale formulation development is conventionally carried out using small-scale internal mixers and two-roll mills. However, high torque laboratory twin-screw micro-compounder, which have been serving the plastic industry for more than 30 years, can be used to formulate new rubber compounds for fast and accurate sample preparation that on top can contribute to the economics of R&D. In this study, we investigated the possibility of using lab-scale 15 mL high torque twin-screw micro-compounder as a tool for new rubber compound development. For this purpose, we formulated EPDM/carbon black and EPDM/silica recipes through conventional way using a Banbury mixer followed by a two-roll mill, and through the possible way using a lab-scale 15 mL twin-screw micro-compounder. We crosslinked both systems via hot press at a predefined temperature and time. The rheological and mechanical properties of the compounds were investigated. Moreover, the dispersion of carbon black and silica in the EPDM matrix was judged by DisperGrader and scanning electron microscope (SEM). The conventional way of sample preparation was compared with a possible sample preparation method based on materials’ parameters and ease of operation.