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Structural, morphological and electrical properties of La1-xSrxAlO3-delta(x=0, 0.1, 0.15) synthesized by the Pechini method

Bouremmad, Farida and Benabbas, Abderrahim and Bouridah, Hachemi and Rida, Kamel and Shawuti, Shalima and Gülgün, Mehmet Ali (2012) Structural, morphological and electrical properties of La1-xSrxAlO3-delta(x=0, 0.1, 0.15) synthesized by the Pechini method. Acta Chimica Slovenica, 59 (4). pp. 927-933. ISSN 1318-0207 (Print) 1580-3155 (Online)

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Abstract

La1-xSrxAlO3-delta (x = 0, 0.1, 0.15) fine particles were prepared by the Pechini process using citric acid and ethylene glycol at low temperature 900 degrees C. The powders were studied by several physical characterization techniques. The FTIR spectrum of the resin treated at 200 degrees C revealed the formation of a metalorganic complex and a polymerized form of ethylene glycol. XRD spectra of the samples, calcined at 900 degrees C, illustrated a single phase LaAlO3. However, La0.9Sr0.1AlO3-delta and La0.85Sr0.15AlO3-delta powders mainly consist of a deficient hexagonal perovskite phase with a small amount of a second phase (LaSrAl3O7). Ionic conductivities of these materials were studied by impedance spectroscopy in the range of 100-700 degrees C in air.

Item Type:Article
Additional Information:Listed in: DOAJ as an open access journal
Uncontrolled Keywords:Ionic conductivity; sol gel; solid oxide fuel cell; impedance spectroscopy; perovskite
Subjects:Q Science > QD Chemistry
ID Code:24208
Deposited By:Mehmet Ali Gülgün
Deposited On:09 May 2014 15:00
Last Modified:09 May 2014 15:00

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